HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11321766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Fluoro-11-[beta-(dimethylamino) ethoxy]dibenz[b,f]oxepin | HCID 19760519 | — |
| Product | HCID 11321766 | HCID 11321766 | — |
Reaction Steps
Reflux of 25 ml of 2-fluoro-11-[β-(dimethylamino)-ethoxy]dibenz[b,f]oxepin stock solution produced no apparent decomposition after 45 minutes. Addition of 2.5 ml of concentrated hydrochloric acid and further reflux for 10 mins gave complete decomposition to 10,11-dihydro-10-oxodibenz[b,f]oxepin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05140027 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-33922ff8400349039e373c01f6de26c7 |
| Source note | uspto-grants-1992_08 |