HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → Ethyl 4-[2-(4-cyanobenzenesulphonylamino)-ethyl]-cyclohexylacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Cyanobenzenesulfonyl chloride | HCID 39497 | — |
| Reactant | HCID 67807757 | HCID 67807757 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Ethyl 4-[2-(4-cyanobenzenesulphonylamino)-ethyl]-cyclohexylacetate | HCID 20078478 | 95% |
Reaction Steps
by the reaction of 4-cyanobenzenesulphonyl chloride with ethyl 4-(2-aminoethyl)-cyclohexylacetate hydrochloride in methylene chloride in the presence of triethylamine. Yield 95% of theory, colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05140038 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-8d76213fc8a14a64962dae70317a9d1a |
| Source note | uspto-grants-1992_08 |