1-Oxo-1,2,3,4-tetrahydrophenanthrene → HCID 348924, compound

Participants

Reaction Steps

To a solution of 1,2,3,4-tetrahydrophenanthren-1-one (1.0 g, 5.1 mmol) in pyridine was added hydroxylamine hydrochloride (0.69 g, 10.0 mmol). The resulting mixture was stirred at room temperature overnight. The solvent was removed in vacuo. Water was added to the residue, which was then filtered and dried to provide the oxime.

Provenance & Evidence