HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Iodosuccinimide → HCID 15029852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Iodosuccinimide | HCID 120273 | — |
| Reactant | 5-Hydroxy-1-indanone | HCID 233147 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15029852 | HCID 15029852 | — |
Reaction Steps
5-Hydroxy-1-indanone (1.48 g), N-iodosuccinimide (2.25 g) and CH3CN (20 ml) were stirred at room temperature overnight. The solution was evaporated to dryness, slurried with EtOAc, then filtered. The filtrate was evaporated to dryness and the solid recrystallized from CH3CN affording the desired compound (0.92 g), m.p. 114°-15° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05140040 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-efb52517f643423d880d3e33032187f6 |
| Source note | uspto-grants-1992_08 |