HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15657729, compound → HCID 13202691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15657729 | HCID 15657729 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13202691 | HCID 13202691 | 88% |
Reaction Steps
A solution of the product from Example 4 (27.4 g, 0.120 mol) in methanol was hydrogenated over 5% palladium on carbon (2.5 g). The reaction mixture was concentrated to give the title compound (24.3 g, 88%) as a white solid mp 142°-144° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05141934 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-9490bb7d891945de9fc09439c43f9e1b |
| Source note | uspto-grants-1992_08 |