HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dodecylamine → HCID 13651083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dodecylamine | HCID 13583 | — |
| Reactant | 2-Naphthalenecarboxylic acid, 1,4-dihydroxy-, phenyl ester | HCID 604249 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 13651083 | HCID 13651083 | — |
Reaction Steps
2-phenoxycarbonyl-1,4-dihydroxynaphthalene (28 g) was suspended in acetonitrile (150 ml) and laurylamine (22.2 g) was dropwise added. The resulting mixture was refluxed for 4 hours. After completion of the reaction, the reaction mixture was cooled and the produced crystals were filtered off. (Yield: 26.8 g)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05142029 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-43f1de3965804dbea30b9d33f7ebd8ef |
| Source note | uspto-grants-1992_08 |