HRID847428

反应详情

EQUATION

反应方程式

HRID 847428 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-phenoxycarbonyl-1,4-dihydroxynaphthalene (28 g) was suspended in acetonitrile (150 ml) and laurylamine (22.2 g) was dropwise added. The resulting mixture was refluxed for 4 hours. After completion of the reaction, the reaction mixture was cooled and the produced crystals were filtered off. (Yield: 26.8 g)

WORKUP

后处理

  1. temperatureThe resulting mixture was refluxed for 4 hours
  2. customAfter completion of the reaction
  3. temperaturethe reaction mixture was cooled
  4. filtrationthe produced crystals were filtered off