HRID847428
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
2-phenoxycarbonyl-1,4-dihydroxynaphthalene (28 g) was suspended in acetonitrile (150 ml) and laurylamine (22.2 g) was dropwise added. The resulting mixture was refluxed for 4 hours. After completion of the reaction, the reaction mixture was cooled and the produced crystals were filtered off. (Yield: 26.8 g)
WORKUP
后处理
- temperatureThe resulting mixture was refluxed for 4 hours
- customAfter completion of the reaction
- temperaturethe reaction mixture was cooled
- filtrationthe produced crystals were filtered off