Dodecylamine → HCID 13651083, compound

HRID 847428Notes

Reaction equation

HRID 847428 reaction equation
O([C:8]([C:10]1[CH:19]=[C:18]([OH:20])[C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[C:11]=1[OH:21])=[O:9])C1C=CC=CC=1.[CH2:22]([NH2:34])[CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33]>C(#N)C>[CH2:22]([NH:34][C:8]([C:10]1[CH:19]=[C:18]([OH:20])[C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[C:11]=1[OH:21])=[O:9])[CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33]

Participants

4

Reactant 2

HCID 13583DodecylamineHCID 6042492-Naphthalenecarboxylic acid, 1,4-dihydroxy-, phenyl ester

Product 1

HCID 13651083HCID 13651083, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

2-phenoxycarbonyl-1,4-dihydroxynaphthalene (28 g) was suspended in acetonitrile (150 ml) and laurylamine (22.2 g) was dropwise added. The resulting mixture was refluxed for 4 hours. After completion of the reaction, the reaction mixture was cooled and the produced crystals were filtered off. (Yield: 26.8 g)

Workup

  1. temperatureThe resulting mixture was refluxed for 4 hours
  2. customAfter completion of the reaction
  3. temperaturethe reaction mixture was cooled
  4. filtrationthe produced crystals were filtered off

Sources & evidence

ORD record
ord-43f1de3965804dbea30b9d33f7ebd8ef
Source dataset
uspto-grants-1992_08
Patent number
US05142029

Reaction notes

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