HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → (Cyclohexyloxy)trimethylsilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Cyclohexanol | HCID 7966 | — |
| Catalyst | Tetrabutylammonium Bromide | HCID 74236 | — |
| Product | (Cyclohexyloxy)trimethylsilane | HCID 262864 | — |
Reaction Steps
1 mole of cyclohexanol, 1.5 moles of trimethylchorosilane and 0.0005 moles of tetra-n-butyl ammonium bromide were reacted at the reflux temperature (54°-97° C.) as in Example 1 and then worked up by distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05142081 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-b2a40950a53b4bc1828648cbee2a62b4 |
| Source note | uspto-grants-1992_08 |