Chlorotrimethylsilane → HCID 11809862, compound

HRID 847484Notes

Reaction equation

HRID 847484 reaction equation
[CH2:1]([C:3]([CH2:8][OH:9])([CH2:6][OH:7])[CH2:4]C)[OH:2].[CH3:10][Si:11]([CH3:14])([CH3:13])Cl>[Cl-].C([N+](CC)(CC)CC1C=CC=CC=1)C>[CH3:10][Si:11]([CH3:14])([CH3:13])[O:2][CH2:1][C:3]([CH2:8][O:9][Si:11]([CH3:14])([CH3:13])[CH3:10])([CH3:4])[CH2:6][O:7][Si:11]([CH3:14])([CH3:13])[CH3:10]

Participants

4

Reactant 2

HCID 6397ChlorotrimethylsilaneHCID 6510Trimethylolpropane

Product 1

HCID 11809862HCID 11809862, compound

Reagents, catalysts & solvents 1

HCID 66133Benzyl triethylammonium chlorideCatalyst

Procedure

1 mole of trimethylol propane, 4 moles of trimethylchlorosilane and 0.003 moles of triethylbenzyl ammonium chloride were reacted at the reflux temperature (54°-104° C.) as in Example 1 and then worked up by distillation.

Workup

  1. distillationworked up by distillation

Sources & evidence

ORD record
ord-aba0d9ca83db476eb62f7bed6c86873e
Source dataset
uspto-grants-1992_08
Patent number
US05142081

Reaction notes

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