HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → HCID 11788946, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | alpha-Isopropylacrylic acid | HCID 12122615 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 11788946 | HCID 11788946 | — |
Reaction Steps
α-Isopropylacrylic acid (13 mmol) in dry ether (40 ml) was treated with dicyclohexylcarbodiimide (12 mmol), benzyl alcohol (12 mmol) and 4-dimethylaminopyridine (2.5 mmol). After stirring at ambient temperature for 44 h, the mixture was filtered and evaporated. Silica gel chromatography provided the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05142056 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-f456031dd19d466e80dd8f974a02821e |
| Source note | uspto-grants-1992_08 |