Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chloral | HCID 6407 | — |
| Reactant | HCID 22411782 | HCID 22411782 | — |
| Product | HCID 20566771 | HCID 20566771 | — |
Reaction Steps
To 98.4 g (0.6 mole) of 1,3-bis(2-hydroxyethyl)-thiourea at 65° C. was slowly added 182 g (1.24 moles) of chloral while the temperature was maintained below 75° C. by means of external cooling. The reaction mixture was vigorously stirred and heated at 80° C. for 1 hour. On cooling 275 g of a viscous syrupy product was isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04293454 |
|---|
| Source dataset | uspto-grants-1981_10 |
|---|
| ORD ID | ord-4dfb0bb55e5248d8b94b4fb74bc41409 |
|---|
| Source note | uspto-grants-1981_10 |
|---|
