Hydrogen Peroxide → HCID 20566778, compound

HRID 847665Notes

Reaction equation

HRID 847665 reaction equation
[CH2:1]([P:4]([CH2:9][CH2:10][CH3:11])[CH2:5][CH2:6][C:7]#[N:8])[CH2:2][CH3:3].[OH:12]O>C(O)(=O)C>[C:7]([CH2:6][CH2:5][P:4](=[O:12])([CH2:1][CH2:2][CH3:3])[CH2:9][CH2:10][CH3:11])#[N:8]

Participants

4

Reactant 2

HCID 784Hydrogen PeroxideHCID 54466378HCID 54466378, compound

Product 1

HCID 20566778HCID 20566778, compoundYield 100.2%

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Conditions

Temperature
75 °C

Procedure

To dipropyl cyanoethyl phosphine (6.88 grams, 0.04 mole) in 25 ml glacial acetic acid was added 5.67 grams (0.05 mole) of 30% hydrogen peroxide at 60° C. The reaction mixture was heated for 30 minutes at 75° C. to give 7.5 grams of product.

Sources & evidence

ORD record
ord-0edd8c1fa36b407ab3c97b289ff2d8da
Source dataset
uspto-grants-1981_10
Patent number
US04293464

Reaction notes

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