Potassium Carbonate → HCID 3058924, compound

HRID 847720Notes

Reaction equation

HRID 847720 reaction equation
Cl.[CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[C:12]([CH2:14][CH2:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)=[O:13].C(=O)([O-])[O-].[K+].[K+]>CCOCC>[CH:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][C:3]=1[C:12]([CH2:14][CH2:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)=[O:13]

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 30589231-Propanone, 3-(1H-imidazol-1-yl)-1-(2-naphthalenyl)-, monohydrochloride

Product 1

HCID 3058924HCID 3058924, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

1-[2-(2-Naphthoyl)ethyl]imidazole hydrochloride (1.0 g.) suspended in 50 ml of ether is stirred with excess dilute aqueous potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 1-[2-(2-naphthoyl)ethyl]imidazole.

Workup

  1. dissolutionis completely dissolved
  2. customThe organic layer is then separated
  3. washwashed twice with water
  4. dry with materialdried over magnesium sulfate
  5. customevaporated

Sources & evidence

ORD record
ord-0477174d8bff48629fbfe0832bec4191
Source dataset
uspto-grants-1981_10
Patent number
US04293561

Reaction notes

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