Potassium Carbonate → HCID 178433288, compound

HRID 847919Notes

Reaction equation

HRID 847919 reaction equation
C(=O)([O-])[O-].[K+].[K+].Cl.Cl.[CH3:9][C:10]1[N:11]=[CH:12][NH:13][C:14]=1[CH2:15][S:16][CH2:17][CH2:18][NH2:19]>O>[CH3:9][C:10]1[N:11]=[CH:12][NH:13][C:14]=1[CH2:15][S:16][CH2:17][CH2:18][NH2:19]

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 30159992-(((5-Methyl-1H-imidazol-4-yl)methyl)thio)ethylamine dihydrochloride

Product 1

HCID 178433288HCID 178433288, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Potassium carbonate (7.75 g.) was added to a solution of 4-methyl-5-[(2-aminoethyl)thiomethyl]imidazole dihydrochloride (14.6 g.) in water (120 ml.). The solution was stored at room temperature for 15 minutes, then evaporated to dryness, extracted with isopropyl alcohol and the extracts are concentrated to dryness to give 4-methyl-5-[(2-aminoethyl)thiomethyl]imidazole.

Workup

  1. customevaporated to dryness
  2. extractionextracted with isopropyl alcohol
  3. concentrationthe extracts are concentrated to dryness

Sources & evidence

ORD record
ord-b73d55a6d2bd48a08fc3d83505e5ce07
Source dataset
uspto-grants-1981_10
Patent number
US04293699

Reaction notes

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