HRID84800

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)(C)OC(=O)N[C@H]1CCCC[C@H]1Nc1ccc(C(N)=O)c(Nc2cc(-c3ccccc3)no2)c1

HCID69284828

未命名化合物

PRODUCTS

生成物

结构：NC(=O)c1ccc(N[C@@H]2CCCC[C@@H]2N)cc1Nc1cc(-c2ccccc2)no1

HCID57334184

未命名化合物

收率 20.9%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6422

未命名化合物

PROCEDURE

实验过程

Compound tert-butyl (1S,2R)-2-(4-carbamoyl-3-(3-phenylisoxazol-5-ylamino)phenylamino)cyclohexylcarbamate (6 mg) was dissolved in TFA (1 mL). After 10 min of standing, TFA removed in vacuo. The residue was purified by HPLC to give the titled compound (1 mg). MS 392.4 (M+H); UV 202.9, 294.0 nm

WORKUP

后处理

customAfter 10 min of standing, TFA removed in vacuo
customThe residue was purified by HPLC