HRID848071

反应详情

EQUATION

反应方程式

HRID 848071 的结构方程式

PROCEDURE

实验过程

8.6 g of methyl acrylate are added dropwise to 5.9 g of isopropylamine under ice-cooling and stirring. The mixture is further stirred at room temperature for 5 hours. Then, the reaction mixture is distilled under reduced pressure. 12.3 g of methyl 3-isopropylaminopropionate are thereby obtained as a colorless oil. Yield: 84.5%

WORKUP

后处理

  1. temperaturecooling
  2. stirringThe mixture is further stirred at room temperature for 5 hours
  3. distillationThen, the reaction mixture is distilled under reduced pressure