HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → Methyl α-(2-benzothiazolylthio)benzeneacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 3871316 | HCID 3871316 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Methyl α-(2-benzothiazolylthio)benzeneacetate | HCID 54106029 | — |
Reaction Steps
1 g of 2-(benzothiazol-2-ylthio)-2-phenylacetic acid is dissolved in 20 ml of THF, an ethereal solution of diazomethane is added dropwise until a yellow coloration is produced and the mixture is evaporated to give 2-(benzothiazol-2-ylthio)-2-phenylacetic acid methyl ester, in the form of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294839 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-f533ebbf28634df398ccea1fbf32eaee |
| Source note | uspto-grants-1981_10 |