HuagongsheHuagongshe Chemistry Print Report · For research reference only
4'-Fluoroacetophenone → HCID 53830815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4'-Fluoroacetophenone | HCID 9828 | — |
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Tetramethylammonium hydroxide | HCID 60966 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53830815 | HCID 53830815 | — |
Reaction Steps
The procedure is as in Example 11 starting from 2.9 g of 4-fluoroacetophenone and 3 g of pyridine-4-carbaldehyde, but using a solution of tetramethylammonium hydroxide in methanol instead of the aqueous solution of sodium hydroxide. 1-(4-fluorophenyl) 3-(4-pyridyl) 2-propene-1-one which melts at 157° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294841 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-e057ccec77f0409fada9753a1699ad43 |
| Source note | uspto-grants-1981_10 |