HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 54267340, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Methoxy-1-phenylethanone | HCID 77698 | — |
| Product | HCID 54267340 | HCID 54267340 | — |
Reaction Steps
The procedure is as in Example 11, starting from 15 g of 2-methoxyacetophenone and 20.4 g of pyridine-4-carbaldehyde in 50 ml of methanol and using 45 ml of a 2.5 N aqueous sodium hydroxide solution in place of the 11 N solution. 7 g of 1-(2-methoxyphenyl) 3-(4-pyridyl) 2-propene-1-one which melts at 70° C. are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294841 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-7a23613ecdcd48d3b236ee4155a61aba |
| Source note | uspto-grants-1981_10 |