HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20566347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | Benzenamine, 2-((1,2,4-oxadiazol-3-ylmethyl)thio)- | HCID 3057622 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 20566347 | HCID 20566347 | — |
Reaction Steps
Methanesulphonyl chloride (1.39 g) was added dropwise to a cooled solution of 3-(2-aminophenylthiomethyl)-1,2,4-oxadiazole (3.1 g) in pyridine (12 ml). The reaction mixture was then poured into water (75 ml) the so formed solid removed by filtration and crystallised from ethanol to give 3-(2-methylsulphonamidophenylthiomethyl)-1,2,4-oxadiazole, m.p. 106°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294843 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-7d0737f2ea4f42e69f5b2de7e77e5887 |
| Source note | uspto-grants-1981_10 |