Benzene → HCID 54574710, compound

Participants

Reaction Steps

Phenylisothiocyanate (1.31 g) in benzene (10 ml) was added dropwise to a stirred solution of 3-(2-aminophenylthiomethyl)-1,2,4-oxadiazole (20 g) in benzene (10 ml). The resultant solution was refluxed for 3 hours, the solvent removed by evaporation under reduced pressure to give a solid which was re-crystallised from isopropanol to give N-[2-(1,2,4-oxadiazol-3-yl-methylthio)phenyl]-N1 -phenylthiourea, m.p. 128°.

Provenance & Evidence