HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl glycidyl ether → HCID 20566365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl glycidyl ether | HCID 31217 | — |
| Reactant | Benzenamine, 2-((1,2,4-oxadiazol-3-ylmethyl)thio)- | HCID 3057622 | — |
| Product | HCID 20566365 | HCID 20566365 | — |
Reaction Steps
A mixture of 3-(2-aminophenylthiomethyl)1,2,4-oxadiazole (2.07 g; 10-2 mol) and 1,2-epoxy-3-phenoxy propane (1.5 g; 10-2 mol) was warmed on a steam bath during 48 hours. The so produced mixture was chromatographed on silica gel, elution with diethyl ether/hexane (1:1) producing 2-hydroxy-1-[2-(1,2,4-oxadiazol-3-yl-methylthio)anilino]-3-phenoxypropane as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294843 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-5dd18a6e32de4b42a97e22bb18fc1e61 |
| Source note | uspto-grants-1981_10 |