Hydrochloric Acid → HCID 70563461, compound

HRID 848396Notes

Reaction equation

HRID 848396 reaction equation
C([NH:4][C:5]1[CH:21]=[CH:20][C:8]([N:9]([CH2:17][CH2:18][OH:19])[CH2:10][CH2:11][NH:12][S:13]([CH3:16])(=[O:15])=[O:14])=[CH:7][CH:6]=1)(=[O:3])C.[ClH:22]>O>[OH2:3].[ClH:22].[ClH:22].[OH:19][CH2:18][CH2:17][N:9]([CH2:10][CH2:11][NH:12][S:13]([CH3:16])(=[O:15])=[O:14])[C:8]1[CH:7]=[CH:6][C:5]([NH2:4])=[CH:21][CH:20]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 20565165HCID 20565165, compound

Product 1

HCID 70563461HCID 70563461, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

0.0178 mol (5.6 g) of 4-acetylamino-N-(β-hydroxyethyl)-N-(β-mesylaminoethyl)-aniline in 12 ml of a 5 N aqueous solution of hydrochloric acid is heated for 30 minutes in a boiling water bath. The water is then driven off in vacuo. After keeping the residue for two hours in vacuo at 60° C., a crystalline product, which is chromatographically pure, is obtained.

Workup

  1. customfor two hours
  2. customat 60° C.
  3. customis obtained

Sources & evidence

ORD record
ord-feb4f3ed41894d3082458b4c15251618
Source dataset
uspto-grants-1981_10
Patent number
US04295848

Reaction notes

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