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HRID848449

反应详情

EQUATION

反应方程式

HRID 848449 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CSC(CSC(C)=O)C(=O)O
HCID20539692

未命名化合物

PRODUCTS

生成物

1
结构：CSC(CSC(C)=O)C(=O)Cl
HCID54341183

未命名化合物

PROCEDURE

实验过程

The 3-(acetylthio)-2-(methylthio)propionic acid is refluxed in thionyl chloride for two hours. The reaction mixture is distilled to remove excess thionyl chloride and the product is distilled in vacuo to yield 3-(acetylthio)-2-(methylthio)propionic acid chloride.

WORKUP

后处理

  1. distillationThe reaction mixture is distilled
  2. customto remove excess thionyl chloride
  3. distillationthe product is distilled in vacuo