HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-(Acetylthio)-2-(methylthio)propionic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(Acetylthio)-2-(methylthio)propionic acid | HCID 20539692 | — |
| Product | 3-(Acetylthio)-2-(methylthio)propionic acid chloride | HCID 54341183 | — |
Reaction Steps
The 3-(acetylthio)-2-(methylthio)propionic acid is refluxed in thionyl chloride for two hours. The reaction mixture is distilled to remove excess thionyl chloride and the product is distilled in vacuo to yield 3-(acetylthio)-2-(methylthio)propionic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04296113 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-bd32fff80e9849688a264e32c4cdfb35 |
| Source note | uspto-grants-1981_10 |