huagongshe.com
HRID848462

反应详情

EQUATION

反应方程式

HRID 848462 的结构方程式

REACTANTS

反应物

2
结构：C=[N+]=[N-]
HCID9550

Diazomethane

CH2N2

结构：CC(=O)SCCC(=O)N1CC(=O)C[C@H]1C(=O)O
HCID12773663

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)[C@@H]1CC(=O)CN1C(=O)CCSC(C)=O
HCID12773675

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

A solution of the product of Example 1 in ether is treated with a slight excess of diazomethane. After standing at room temperature for two hours, the solvent is evaporated to give 1-[3-(acetylthio)-1-oxopropyl]-4-oxo-L-proline, methyl ester.

WORKUP

后处理

  1. customthe solvent is evaporated