Ethyl pyruvate → HCID 20565446, compound
Reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]2[C:10]([NH2:16])=[CH:11][C:12]([CH3:15])=[CH:13][CH:14]=2)=[CH:4][CH:3]=1.[C:17](OCC)(=[O:21])[C:18]([CH3:20])=O>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:9]3[C:10](=[CH:11][C:12]([CH3:15])=[CH:13][CH:14]=3)[N:16]=[C:18]([CH3:20])[C:17]2=[O:21])=[CH:4][CH:3]=1Participants
3
Procedure
Preparation as in Example 1 but using N-(4-chlorophenyl)-4-methylbenzene-1,2-diamine and ethyl pyruvate gave the title compound mp 223°-225° C.
Workup
- customPreparation as in Example 1
Sources & evidence
- ORD record
- ord-07566581118e4ee08e7bcaddc0f20bd9
- Source dataset
- uspto-grants-1981_10
- Patent number
- US04296114
Reaction notes
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