Ethyl pyruvate → HCID 20565467, compound
Reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]2[C:10]([NH2:16])=[CH:11][CH:12]=[C:13]([CH3:15])[CH:14]=2)=[CH:4][CH:3]=1.[C:17](OCC)(=[O:21])[C:18]([CH3:20])=O>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:9]3[C:10](=[CH:11][CH:12]=[C:13]([CH3:15])[CH:14]=3)[N:16]=[C:18]([CH3:20])[C:17]2=[O:21])=[CH:4][CH:3]=1Participants
3
Procedure
Preparation as in Example 1 but using N-(4-chlorophenyl)-5-methylbenzene-1,2-diamine and ethyl pyruvate gave the title compound mp 144°-145° C.
Workup
- customPreparation as in Example 1
Sources & evidence
- ORD record
- ord-7706f974b7284f9985507fab8c7b9653
- Source dataset
- uspto-grants-1981_10
- Patent number
- US04296114
Reaction notes
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