HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,5,6(1H,3H)-Pyrimidinetetrone, monohydrate → HCID 56633917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,5,6(1H,3H)-Pyrimidinetetrone, monohydrate | HCID 16723 | — |
| Reactant | HCID 3837384 | HCID 3837384 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 56633917 | HCID 56633917 | — |
Reaction Steps
To a solution of N-(4-methoxyphenyl)benzene-1,2-diamine (9.0 g) in ethanol (150 ml) was added a solution of alloxan monohydrate (6.7 g) in water (150 ml) and the mixture was stirred for 30 minutes. The precipitate was filtered off and recrystallised from glacial acetic acid giving the title compound mp 236°-238° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04296114 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-62625e2fe9614868958e51327dbb292d |
| Source note | uspto-grants-1981_10 |