HRID848574

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID3283

Diethyl Ether

C4H10O

3 次

HCID8471

Triethylamine

C6H15N

HCID6918953

未命名化合物

结构：CC(C)(Oc1ccc(C(=O)c2ccc(Cl)cc2)cc1)C(=O)Cl

HCID19025865

2-[4-(4-Chlorobenzoyl)phenoxy]-2-methylpropanoyl chloride

C17H14Cl2O3

PRODUCTS

生成物

结构：CC(C)(Oc1ccc(C(=O)c2ccc(Cl)cc2)cc1)C(=O)N(CCO)CCO.CC(C)(Oc1ccc(Cl)cc1)C(=O)O.CC(C)(Oc1ccc(Cl)cc1)C(=O)O

HCID20398478

未命名化合物

PROCEDURE

实验过程

A solution of 1.948 g (5.8 millimoles) of 2-(4-(4-chlorobenzoyl)-phenoxy)-2-methyl propanoyl chloride in 10 ml of methylic ether was slowly added to a solution containing ether was slowly added to a solution containing 2.9 g (5.8 millimoles) of amino diethyl bis-2-(4-chlorophenoxy)-2-methylpropanoate (prepared according to French Pat. No. 2,085,634) and 0.83 ml (6 millimoles) of triethylamine in 30 ml of ethylic ether kept at 0° C.

WORKUP

后处理

additionwas slowly added to a solution
customprepared
customkept at 0° C.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-d2a3ebdea2484374a577151f368e3765
来源数据集: uspto-grants-1981_10
DOI: 10.6084/m9.figshare.5104873.v1
专利: US04296125
来源说明: uspto-grants-1981_10

反应 SMILES

[Cl:1][C:2]1[CH:22]=[CH:21][C:5]([C:6]([C:8]2[CH:20]=[CH:19][C:11]([O:12][C:13]([CH3:18])([CH3:17])[C:14](Cl)=[O:15])=[CH:10][CH:9]=2)=[O:7])=[CH:4][CH:3]=1.[Cl:23][C:24]1[CH:36]=[CH:35][C:27]([O:28][C:29]([CH3:34])([CH3:33])[C:30]([O-:32])=[O:31])=[CH:26][CH:25]=1.[CH2:37]([N:39](CC)CC)[CH3:38].CC[O:46][CH2:47][CH3:48]>>[Cl:23][C:24]1[CH:25]=[CH:26][C:27]([O:28][C:29]([CH3:34])([CH3:33])[C:30]([OH:32])=[O:31])=[CH:35][CH:36]=1.[Cl:23][C:24]1[CH:25]=[CH:26][C:27]([O:28][C:29]([CH3:34])([CH3:33])[C:30]([OH:32])=[O:31])=[CH:35][CH:36]=1.[Cl:1][C:2]1[CH:22]=[CH:21][C:5]([C:6]([C:8]2[CH:20]=[CH:19][C:11]([O:12][C:13]([CH3:18])([CH3:17])[C:14]([N:39]([CH2:48][CH2:47][OH:46])[CH2:37][CH2:38][OH:28])=[O:15])=[CH:10][CH:9]=2)=[O:7])=[CH:4][CH:3]=1