HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86738063, compound → HCID 86738066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86738063 | HCID 86738063 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86738066 | HCID 86738066 | 45.7% |
Reaction Steps
To a solution of trans, trans-2,4-nonadien-1-ol (20 g) in chloroform (400 ml) was added manganese dioxide (125 g). The mixture was stirred for 11 hours at ambient temperature and then filtered. The filtrate was concentrated under reduced pressure to give an oily residue, which was subjected to a column chromatography on silica gel (developing solvent: chloroform). The eluate was concentrated under reduced pressure to give colorless oily trans, trans-2,4-nonadienal (9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04297096 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-9941ce206cff4f14aaf6db444c754b16 |
| Source note | uspto-grants-1981_10 |