HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86738067, compound → HCID 86738070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86738067 | HCID 86738067 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86738070 | HCID 86738070 | — |
Reaction Steps
To a solution of trans, trans, trans-2,4,6-undecatrien-1-ol (7.2 g) in chloroform (300 ml) was added manganese dioxide (50 g) and then the mixture was stirred for 15 hours at ambient temperature. The resultant mixture was filtered and the filtrate was concentrated under reduced pressure to give an oily residue, which was subjected to a column chromatography on silica gel (developing solvent: chloroform). The eluate was concentrated under reduced pressure to give oily trans, trans, trans-2,4,6-undecatrienal (5.5. g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04297096 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-fa87428232d441e2be2380ca12c4839d |
| Source note | uspto-grants-1981_10 |