HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluoroaniline → HCID 70547182, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluoroaniline | HCID 9742 | — |
| Reactant | ethyl N-(2-cyano-3-ethoxyacryloyl)carbamate | HCID 230015 | — |
| Product | HCID 70547182 | HCID 70547182 | — |
Reaction Steps
3-Fluoroaniline (0.05 mol) is reacted with α-cyano-β-ethoxy-N-ethoxycarbonylacrylamide (0.05 mol) to yield α-cyano-β-(3-fluoroanilino)-N-ethoxycarbonylacrylamide, m.p. 169.5°-171.0°, which is heated at reflux in tetralin to yield 5-cyano-1-(3-fluorophenyl)uracil, m.p. 245.5°-246.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04297297 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-abbda641fdcb4c4b9440402fe091f25f |
| Source note | uspto-grants-1981_10 |