HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20564189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 20564185 | HCID 20564185 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 20564189 | HCID 20564189 | — |
Reaction Steps
Suspend 7-carboxy-(1H,3H,5H)-(1)-benzopyrano-(2,3-d)-pyrimidine-4-one-2-thione (5 g.) in ethanol and pass in HCl gas until saturated. Reflux the mixture for 24 hours then cool, filter and wash with ethanol and ether to yield 7-ethoxycarbonyl(1H,3H,5H)-(1)-benzopyrano-(2,3-d)-pyrimidine-4-one-2-thione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04297355 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-8b4a2aadaeb5419c99c0822f92f09363 |
| Source note | uspto-grants-1981_10 |