HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 20564655, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | 2-((2-(Ethylthio)ethyl)thio)amine | HCID 20521802 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 20564655 | HCID 20564655 | — |
Reaction Steps
6 g of methyl isocyanate in 15 ml of ethyl acetate were added dropwise at room temperature to a solution of 16.5 g of 1-amino-3,6-dithiaoctane in 40 ml of ethylacetate. The urea precipitated was recrystallised twice from methanol/water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04297439 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-98b0d249dda34bff9b31a6ece2bf5710 |
| Source note | uspto-grants-1981_10 |