2-Amino-2-methyl-1,3-propanediol → N-(1,3-Dihydroxy-2-methylpropan-2-yl)-N'-dodecylurea

HRID 848932Notes

Reaction equation

HRID 848932 reaction equation
[NH2:1][C:2]([CH3:7])([CH2:5][OH:6])[CH2:3][OH:4].[CH2:8]([NH:20][C:21](N1C=CN=C1)=[O:22])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]>CO>[CH2:8]([NH:20][C:21]([NH:1][C:2]([CH2:5][OH:6])([CH3:7])[CH2:3][OH:4])=[O:22])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Participants

4

Reactant 2

HCID 15312-Amino-2-methyl-1,3-propanediolHCID 18328494HCID 18328494, compound

Product 1

HCID 15847429N-(1,3-Dihydroxy-2-methylpropan-2-yl)-N'-dodecylurea

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The preparation was carried out, according to the same process described in Example 1, from 3.5 g of 2-amino-2-methyl-1,3-propanediol of corresponding formula R2 --NH--R3, where R2 denoted H and R3 denoted: ##STR7## and 7 g of 1-N-(dodecylaminocarbonyl)imidazole of corresponding formula (III), where R1 denoted C12H25, in 100 cm3 of methanol.

Sources & evidence

ORD record
ord-c1a1f1e548684b9ba816f6c9332d8063
Source dataset
uspto-grants-2000_01
Patent number
US06010707

Reaction notes

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