Phenothiazine → HCID 22118765, compound

HRID 848969Notes

Reaction equation

HRID 848969 reaction equation
[CH:1]1[C:14]2[NH:13][C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[S:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.Br[CH2:16][C:17]1[O:18][C:19]2[CH:25]=[CH:24][C:23]([CH:26]=[O:27])=[CH:22][C:20]=2[CH:21]=1>>[CH:26]([C:23]1[CH:24]=[CH:25][C:19]2[O:18][C:17]([CH2:16][N:13]3[C:14]4[CH:1]=[CH:2][CH:3]=[CH:4][C:5]=4[S:6][C:7]4[C:12]3=[CH:11][CH:10]=[CH:9][CH:8]=4)=[CH:21][C:20]=2[CH:22]=1)=[O:27]

Participants

3

Reactant 2

HCID 7108PhenothiazineHCID 22118749HCID 22118749, compound

Product 1

HCID 22118765HCID 22118765, compoundYield 33.2%

Procedure

The title compound (1.14 g, 33%) was prepared as a syrupy liquid from phenothiazine (2.87 g, 14.0 mmol) and 2-bromomethyl-5-formyl benzofuran (2.3 g, 9.6 mmol) by a similar procedure to that described in preparation 5.

Workup

  1. customthat described in preparation 5

Sources & evidence

ORD record
ord-63a7cbb09d4840be852dc6c0fee3b2fc
Source dataset
uspto-grants-2000_01
Patent number
US06011031

Reaction notes

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