HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10422857, compound → HCID 15411306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10422857 | HCID 10422857 | — |
| Reactant | 7-Amino-2H-1,4-benzothiazin-3(4H)-one | HCID 12627419 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15411306 | HCID 15411306 | 92.5% |
Reaction Steps
A liquid mixture of 1.316 g (5 mmol) of 3-(2-quinolinylmethoxy)benzaldehyde, 0.901 g (5 mmol) of 7-amino-3,4-dihydro-2H-1,4-benzothiazin-3-one and 70 ml of EtOH was heated under reflux and stirring for 24 hours. The mixture was then allowed to cool down. The precipitate was collected by filtration, whereby 1.969 g of the title compound were obtained as pale yellow powder (yield: 92.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06011033 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-e84577f2fabb468f8c81768303a187d3 |
| Source note | uspto-grants-2000_01 |