Potassium Carbonate → HCID 18800716, compound

HRID 849055Notes

Reaction equation

HRID 849055 reaction equation
[C:1]([CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][C:7]1=[O:12])(OCC)=O.C(=O)([O-])[O-].[K+].[K+].BrC[C:21]1[S:22][CH:23]=[CH:24][CH:25]=1>[I-].C([N+](CCCC)(CCCC)CCCC)CCC>[S:22]1[CH:23]=[CH:24][CH:25]=[C:21]1[CH2:1][CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][C:7]1=[O:12]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 95543Ethyl 2-oxocyclohexanecarboxylateHCID 118299782-(Bromomethyl)thiophene

Product 1

HCID 18800716HCID 18800716, compound

Reagents, catalysts & solvents 1

HCID 67553Tetrabutylammonium IodideCatalyst

Procedure

2-carboethoxycyclohexanone, finely powdered potassium carbonate, 2-bromomethyl thiophene, and tetrabutylammonium iodide are reacted by the method of Example 38 to generate the title material.

Sources & evidence

ORD record
ord-fc5b4973e63543dba324fc1db8ab4a10
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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