HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 10560088, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) | HCID 2735153 | — |
| Reactant | HCID 10750163 | HCID 10750163 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10560088 | HCID 10560088 | 73.8% |
Reaction Steps
A solution of the product of Example 62 (400 mg, 2.0 mmol) in methylene chloride (25 mL) was treated with trimethyloxonium tetrafluoroborate (361 mg, 2.4 mmol) by the method of Example 3 to produce the title material (300 mg, 40%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06011028 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-2f82b67687314d40ab624bb4087d1d21 |
| Source note | uspto-grants-2000_01 |