HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178479039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 6-Benzylpyridin-2-amine | HCID 93902 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Product | HCID 178479039 | HCID 178479039 | — |
Reaction Steps
The 2-amino-6-benzylpyridine was reduced as in Example 94, except platinum oxide was used as the catalyst. The product was obtained as an oil which was dissolved in 1 N HCl and lyophilized to give a white solid. The solid was recrystallized from EtOAc to give the desired title compound as white crystals. The analysis of the product was found to be consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06011028 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-ab961bebbe72482badb3276f57ec740a |
| Source note | uspto-grants-2000_01 |