HRID849081

反应详情

EQUATION

反应方程式

HRID 849081 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The 2-amino-6-benzylpyridine was reduced as in Example 94, except platinum oxide was used as the catalyst. The product was obtained as an oil which was dissolved in 1 N HCl and lyophilized to give a white solid. The solid was recrystallized from EtOAc to give the desired title compound as white crystals. The analysis of the product was found to be consistent with the proposed structure.

WORKUP

后处理

  1. customThe product was obtained as an oil which
  2. customto give a white solid
  3. customThe solid was recrystallized from EtOAc