HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Cyanide → 2-[2-(1,3-Dioxan-2-yl)ethyl]cyclohexanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | Methyl 1-[2-(1,3-dioxan-2-yl)ethyl]-2-oxocyclohexanecarboxylate | HCID 18800662 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 2-[2-(1,3-Dioxan-2-yl)ethyl]cyclohexanone | HCID 10798604 | — |
Reaction Steps
The product of Example 108 is reacted with sodium cyanide in DMSO at 160° C. by the method of Example 103 to generate the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06011028 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-df313e06cac54b4fa594ab74ce8608a9 |
| Source note | uspto-grants-2000_01 |