Hydroxyamine hydrochloride → HCID 73517215, compound

HRID 849110Notes

Reaction equation

HRID 849110 reaction equation
O=[C:2]1[CH2:7][CH2:6][CH2:5][CH2:4][CH:3]1[CH2:8][C:9]#[N:10].Cl.[NH2:12][OH:13].C([O-])(=O)C.[Na+]>C(O)C.O>[OH:13][N:12]=[C:2]1[CH2:7][CH2:6][CH2:5][CH2:4][CH:3]1[CH2:8][C:9]#[N:10]

Participants

5

Reactant 3

HCID 443297Hydroxyamine hydrochlorideHCID 517045Sodium AcetateHCID 5435532-Oxocyclohexaneacetonitrile

Product 1

HCID 73517215HCID 73517215, compound

Reagents, catalysts & solvents 1

HCID 19096565Water ethanolSolvent

Procedure

The product of Example 149 is reacted with hydroxylamine hydrochloride and sodium acetate in ethanol/water by the method of Example 1 to generate the title compound.

Sources & evidence

ORD record
ord-e2e7e3abefff4427858389d91b2f4a3c
Source dataset
uspto-grants-2000_01
Patent number
US06011028

Reaction notes

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