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HRID849145

反应详情

EQUATION

反应方程式

HRID 849145 的结构方程式

REACTANTS

反应物

3
结构：O=Cc1ccccc1
HCID240

Benzaldehyde

C7H6O

结构：Nc1ccccc1N
HCID7243

1,2-Phenylenediamine

C6H8N2

结构：O=[N+]([O-])/C=C/c1ccccc1
HCID5284459

(E)-beta-Nitrostyrene

C8H7NO2

PRODUCTS

生成物

1
结构：O=[N+]([O-])CCc1ccccc1
HCID80208

(2-Nitroethyl)benzene

C8H9NO2

收率 95%

PROCEDURE

实验过程

Example 219 A) trans-b-Nitrostyrene (63.0 g, 0.42 mole) was reacted with benzaldehyde (53.4 g, 0.5 mole) and 1,2-diaminobenzene (54.4 g, 0.5 mole) according to the procedure of Chikashita et. al. (Synth. Commun. 1985, 15 (6), 527) to yield (2-nitroethyl)benzene (60.0 g, 95%) as a yellow oil.