HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-1-butanol → HCID 19369795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-1-butanol | HCID 25868 | — |
| Reactant | HCID 11728593 | HCID 11728593 | — |
| Solvent | Diethylene Glycol | HCID 8117 | — |
| Product | HCID 19369795 | HCID 19369795 | — |
Reaction Steps
1-(2-Methylphenyl)-4-chloro-6-trifluoromethoxy-2,3-dihydropyrrolo[3,2-c]quinoline(600 mg, 1.6 mmol) was dissolved in diethylene glycol(10 ml) and hereto was added 4-amino-1-butanol(1.0 ml), then reacted at the same condition of Step 5 in the Example 1 to obtain 510 mg of desired compound as solid in 73% of yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06011044 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-0f41c1767b2742c1b8dc206d5f1b0644 |
| Source note | uspto-grants-2000_01 |