HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19369839, compound → HCID 19369831, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19369839 | HCID 19369839 | — |
| Solvent | 4-Amino-1-butanol | HCID 25868 | — |
| Product | HCID 19369831 | HCID 19369831 | 133.5% |
Reaction Steps
1-(2-methyl-4-fluorophenyl)-4-chloro-6-trifluoromethoxy-2,3-dihydro-pyrrolo[3,2-c]quinoline(500 mg, 1.3 mmol) was dissolved in 4-amino-1-butanol(5 ml) in the pressure tube, then reacted at the same condition of Step 3 in the Example 16 to obtain 390 mg of desired compound as solid in 74% of yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06011044 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-c49af5e12f4c43d49bbc731bb6ae0acf |
| Source note | uspto-grants-2000_01 |