HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Imidazole-4-carbaldehyde → HCID 178478530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Imidazole-4-carbaldehyde | HCID 76428 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 178479668 | HCID 178479668 | — |
| Reactant | HCID 178479669 | HCID 178479669 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178478530 | HCID 178478530 | — |
Reaction Steps
Example 45 was prepared as an off white solid from Compound B of Example 12 as described for Compound D of Example 1, using methylene chloride as solvent, 4.3 equivalents of 4-formylimidazole, 4.3 equivalents of sodium triacetoxyborohydride and with stirring for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06011029 |
| Source dataset | uspto-grants-2000_01 |
| ORD ID | ord-2a2548f2e67d46c08f9cdf0caaead780 |
| Source note | uspto-grants-2000_01 |