HCID 67167490, compound → HCID 67167825, compound

Participants

Reaction Steps

The title compound was prepared as the hydrochloride salt as described in Example 272F substituting the product from Example 280E for the product obtained from Example 272E. 1H NMR (300 MHz, DMSO-d6) δ ppm 1.69-1.86 (m, 1H) 1.86-2.03 (m, 1H) 2.03-2.14 (m, 1H) 2.84-3.03 (m, 1H) 3.12-3.27 (m, 1H) 3.35-3.47 (m, 1H) 3.47-3.63 (m, 2H) 3.64-3.76 (m, 4H) 4.31-4.47 (m, 1H) 6.53-6.73 (m, 2H) 7.00 (d, J=8.33 Hz, 1H) 9.26 (s, 2H); MS (DCI+) m/z 220.1 [M+H]+.

Provenance & Evidence