Hydrochloric Acid → HCID 67167889, compound

HRID 84971Notes

Reaction equation

HRID 84971 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4](/[CH:8]=[CH:9]/[N+:10]([O-:12])=[O:11])[C:3]=1[O:13]COC.Cl>CO.O1CCOCC1>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4](/[CH:8]=[CH:9]/[N+:10]([O-:12])=[O:11])[C:3]=1[OH:13]

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 67167305HCID 67167305, compound

Product 1

HCID 67167889HCID 67167889, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 312751,4-DioxaneSolvent

Procedure

To a suspension of Example 383B in methanol (15 mL) was added 4 N HCl in dioxane (1 mL). The mixture was stirred for 4 hours, concentrated, and diluted with water. The precipitates were collected to afford the titled compound.

Workup

  1. concentrationconcentrated
  2. additiondiluted with water
  3. customThe precipitates were collected

Sources & evidence

ORD record
ord-eda001caede046d5b5e12f4a20bc9b01
Source dataset
uspto-grants-2014_09
Patent number
US08846951B2

Reaction notes

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